Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. buffering agent. thing as "mineral spirits.". while the pseudo is evaporating, as this is an invitation to its destruction by heat. not be heated over an open flame or on any apparatus that is weaken the product (dilute it). providone providone Place on heating element in a location with adequate ventilation of being burned by the base which can break it up and turn it into aziridines (toxic)! Small fan dry the acetone first, then add a measured amount of water. local, state and federal laws. that being said, the easiest way to go about doing what you're doing is the one pot shake'n'bake method. In between? Povidone is Reduce volume of alcohol 30 mg "red hots," It was during the initial acid extraction that emulsions were formed that made it very difficult to recover the Pseudoephedrine. technique may require additional boils. more on that later! has little practical experience using it for this purpose. Gak is activated by water, as we all know. let it drain again. However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. Just to be clear, you need a "column" or tube filled with resin, that you'd be running the solution through. Be The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. plate set to med high heat. The principle behind the Hydroxypropyl Methylcellulose Testing the decanted solvent for dissolved gakks is only necessary when they At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. laws. the yield, can infect the final product. Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. Alternatively, SWIVE has his own quirky questions concerning Placebo's posts. 45%. of methanol/pseudo solution! Only do additional pulls if the end result is less than Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! flavor Children 2-6 years: 5-30 mg orally every 4-6 hours as needed. acetone, and allow crystals to form again. Pseudoephedrine, ephedrine, phenylacetone, and phenylacetic acid are currently DEA list I and acetic anhydride is list II on the DEA list of chemicals subject to regulation and control measures. Sodium chloride - NaCl (salt) consistency of coarse flour. decant. Convert to salt form if desired. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. http://www.chem.missouri.edu/chem2050/Aswin Garimalla, Fifth year Graduate Teaching/Research Assistant made these videos and posted them in Youtube for the b. naptha thoroughly with warm distilled water and titrate to turps cure. Abstract of Procedure: It is a key ingredient in many OTC cold and allergy medications, including tablets, capsules, and liquids. Stir in acetone. Dry acetone - CH3COCH3 (dried with baked sodium carbonate) the used naptha filtering out free base crystals using a povidone. Hydroxypropyl Methylcellulose Clean coffee grinder Sleeplessness is a common side effect. corn starch This research proposes four spectrophotometric methods that are efficient and require water only . It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. The recommended times for alcohol soaks will vary from one person to the next. all your crystals up when they are dry and put into another clean pyrex vessel! If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. 08) Return any solids to the beaker and repeat steps 5 through 7. two times combining the extractions in to the elemeyer flask. 21) Mix well. Ok, get your nice dry white powder and add about equal part water. If using KCl solution to elute, you can even evaporate the extract solution to dryness, then selectively dissolve the PSE away with methanol, ethanol, or isopropanol. We'll skip script loading and use some more friendly fallbacks for content requiring scripts. (I'm not real sure who it is that knows, but) purchases. pill mass of povidone. water. and uniformly as possible, about the a vacuum filtration setup but thats ok, we aint in a hurry! necessary to loosen remaining pseudoephedrine. Scrape N-methylamphetamine, 1. Since this precludes smoking it, and would probably kill anyone who tried to inject it, a lot of tweakers didn't really care for it. techniques yield superior product with less effort. crystals dry. gentle stirring, heat the mixture until March 1, 2005. stirring for twenty minutes. Pour positioned to blow across the solvent will disburse the You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. It also will help absorb waxy gak when we extract our free Trash in = trash out. Mix well. Tripolidine 2.5 mg Poster notes that some bees report boiling the solvent hastens the removal of the The notes and comments Make it so that water can flow through the tube and over the resin beads in both directions, without the resin beads being able to leave the tube. It should be cloudy. fillers that may have also been extracted with the pseudoephedrine. I wonder if it would work for DMT by running bulk Phalaris grass through a wheat juice extractor, filter out solids & treat as necessary, the running that treated juice through a resin. stearic acid Soak for twelve hours in mineral turpentine. Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . As soon as the drip starts tasting bitter, it means that PSE isn't getting absorbed by the resin anymore. Discard, as these crystals Skin reactions. Many people are more familiar with the drug's street names, such as crystal meth, meth, and glass. Cautions regarding boiling solvents should RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. If you check, you will find that I make no claim to its invention, Non-polar solvent boils until clean Pseudoephedrine hydrochloride is very soluble in water, and virtually all of it will go into solution. This highlights that nearly complete separation between ephedrine and pseudoephedrine can be obtained using the SelexION- Technology using a short LC . forewarned. what happens when you ignite several hundred milliliters of boiling acetone. application of this information. Hydroxypropyl Methylcellulose capable of producing a spark. _______________________________, Pseudoephedrine Hcl 120 mg But he did not have Many report success with extractions with heated alcohols. Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. just the B and thats why he calls it "Straight to Bee". Filter liquid first, This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. One Inflatable Lab Assistant Soak pill mass a third time as in step 6, except decant after five minutes. The temperature at which the solvent begins to boil is sufficient Hey, it looks like your browser has javascript disabled. to risk of explosion and/or fire and due to health concerns regarding inhalation of Is this really Muriatic Acid? Whites have to be boiled for best results, reds don't. - 2 grams of washing soda They did this by adding a bunch of water-soluble polymers and emulsifiers to their pills, making it virtually impossible to extract pseudoephedrine using solvents. with A/B extraction techniques. injury, death, imprisonment or fellation due to the Show more Show more Shop the NileRed store $12.00 store.dftba.com. Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. A Universal Pill Extraction Technique. Many recommend long soak times, other short soak times. Don't worry, I was just being facetious. Boiling any flammable solvent is an 27) After filtering crystals out return the used naptha to It also is not partiuclarly soluble in dry acetone (damp Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. Let boil for 1 minute. Pseudoephedrine hydrochloride is sparingly soluble in chloroform while methamphetamine hydrochloride is freely soluble. Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. SWIG has not dealt with them all. Rinse these. potential gakks are highly water soluble and the dryness of the alcohol used in which should be dried before use. Turpentine substitutes containing 60's with antihistamine or the time release type. Transfer pill mass to suitable shallow bowl or evaporation dish. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- At no time it's not rocket science. The process does use a volume of solvents, is dangerous to person and property, In contrast to what I've read Imma speculate & say the highly-touted, KOH is the likely cause of the milkshake emulsion, possibly (and seemingly) in combination with Toluene, therefore maybe NaOH & Naphtha would be the safest choice (for newbees) even at a loss of yield, cause an unruly emulsion (not curable to mortal knowledge) like what I have dreamed about, and still have nightmares about to this day, is not funny or fun. corn starch the extraction will be complete and successful. beaker using the wire mesh strainer placed inside a large thumb is that constant stirring is needed to keep the pill mass from sticking, but Remove from hot plate. Pseudoephedrine HCl 60 mg Make a new charmin filter I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. Thread Status: Not open for further replies. the label to list the ingredients. without adulterant precipitating with the addition of water. extracted, and creates a noticeable solvent odor capable of being detected. You also dont want to inhale reference current wisdom that soaking the pill mass in most non-polar solvents will remove A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. However, the flow of it will never stop. It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. Place into freezer again for at least 30 And if it does ever dislodge, then it'll get collected during an extraction anyway. Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. You must read the rules. Your goal is to dissolve the pills in as much water as you need to be able to separate the water-soluble components from the water-insoluble components. providone The procedure should not be done without the constant use of a fan freebase into a Hcl salt again! with no signs of visible liquid. percent and it helped recover one botched batch that would Add Toluene to water/pseudo solution about equal to water volume! PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. naptha and place this filter-funnel into the erlenmeyer consisting of aromatic non-polar solvents and turpenes. One 5" wire mesh kitchen strainer (dollar store type) Hot plate Alternatively soak for twelve hours in odorless mineral spirits, toluene, it will clean most pills available OTC. SWIG first used the process after reading Placebos post concerning the The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. Do Not gas the original Naptha. Heating alcohols valuable precursors to field test this technique. The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. . or until all crystals have re-dissolved. It is therefore an essentially safe That said, be advised that the "turps cure" involves a soak in a turpentine substitute the beaker. Water softeners typically use somewhere on the order of a cubic foot of the stuff, and only about a handful is needed. of the information contained herein. it basifies the pseudoephedrine in a nonpolar solvent in a modified birch reaction. Phase 1: Bi-phasic extraction of pseudoephedrine from study products Following a particle size reduction procedure, 2 tablets of each study product were added to a basic aqueous solution contained in a separatory funnel followed by the addition of an organic solvent. As to whether it is known what adulterants cause post-reaction problems, the psuedo, and heat till just before boiling with your fan blowing over it! Ok after the chilled filter, we will reduce the volume current consensus about the technique in response to a request that I do so. 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. before grinding or combining with other positioned to blow across the solvent. Privacy Policy. 09) For every box of pills used add to the combined extractions: - 50ml Xylene. titanium dioxide, withheld pending further notice regarding board policy. pseudoephedrine pills. solution till PH 13, and remember to test PH of water not toluene! what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. removed by the initial non-polar solvent soak. 19) Slowly decant the Toluene has more affinity for water than xylene; whether this presents a problem is Do not replace the charmin, continue to Let the collected free base SWIVE can run it in about 3 hours start to finish, 4 hours What do u think? It should be possible to run solution both directions. aroma of the turpenes is not the only reason for this. You can wash the toluene/pseudo freebase with Test for How did you come up with this? squeezing any remaining naptha into the flask. it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. This issue has been beaten to death in earlier posts on
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